MODIFICATION OF GLASS IONOMER CEMENT COMBINED WITH NATURAL NANOSILICA FROM SLOPENG-BEACH SAND TO OPTIMIZE THE MECHANICAL STRENGTH

Fani Pangabdian, Sinta Puspita, Dimas Nugroho, Agung Satria Wardhana, Niesha Amelia

Abstract


Background: Glass Ionomer Cement (GIC) is a restorative material capable of releasing fluoride to protect teeth against the activity of cariogenic bacteria. The use of GIC in restorations has the drawback of low mechanical strength; therefore, material modification is required to optimize its mechanical properties by improving compressive strength, flexural strength, and microhardness, and SEM analysis. Purpose: This study aims to compare the mechanical strength of GIC, GIC combined with synthetic nano-silica, and GIC combined with natural nano-silica from Slopeng Beach sand. Methods: This study comprised 12 groups, each containing 7 samples. The minimum total number of samples required is 84, comprising 28 GIC samples, 28 GIC samples combined with synthetic nano-silica, and 28 GIC samples combined with natural nano-silica from Slopeng Beach sand. Each group will undergo compressive strength, flexural strength, microhardness, and SEM testing.  Results: Compressive Strength Test: K 37.09 ± 16.41 MPa, P1 63.59 ± 12.78 MPa, and P2 51.85 ± 18.38 MPa; Flexural Strength Test: K 23.67 ± 12.88 MPa, P1 34.15 ± 10.42 MPa, and P2 25.47 ± 11.03 MPa; Microhardness Test: K 377.257 ± 69.1203 HV, P1 379.263 ± 60.3404 HV, and P2 384.467 ± 112.4236 HV; SEM results showed that group P1 had a more homogeneous surface morphology with fewer and smaller cracks compared to group P2 and the control (K). Conclusion: GIC combined with nano-silica from Slopeng Beach sand exhibits superior mechanical properties (compressive strength, flexural strength, microhardness, and SEM analysis) compared to GIC combined with synthetic nano-silica.

Keywords


Glass Ionomer Cement; natural nano-silica; compressive strength; flexural strength; microhardness; Scanning Electron Microscopy

Full Text:

PDF

References


Powers JM, Wataha JC, Chen Y-W. Dental Materials: Foundations and Applications, 11th Edition. Vol. 32, The Journal of the Egyptian Medical Association. 2017. pp. 560–568.

McCabe JF, Walls AW. Applied Dental Materials, 9th Edition. 9th ed. Blackwell. Blackwell Munksgaard; 2015. pp. 1–303.

Banerjee A, Watson TF. Pickard’s Guide to Minimally Invasive Operative Dentistry. Pickard’s Guide to Minimally Invasive Operative Dentistry. 2015.

Sakaguchi R, Ferracane J, Powers J. Craig’s Restorative Dental Materials. Fourteenth ed. Elsevier Inc.; 2018. pp. 1–331.

Hinkle J., Shen C., Rawls H.R., and Esquivel-Upshaw J.F. Phillips’ Science of Dental Materials, Elsevier; 2022: 271–286. Cohen’s Pathways Pulp. 2015.

Hidayat R, Yupita, Pangestuti PW, Tafdila NA, Fabiani VA. “Implementasi Matematika dan Sains dalam Teknologi Cerdas untuk Ketahanan Pangan, Energi, dan Kesehatan” Ekstraksi dan Karakterisasi Silika dari Abu Limbah Ampas Tebu Minuman Sari Tebu di Bangka. Pros Semin Nas Sains Dan Terap. 2023;1(November):72–7. Available from: https://ejournal.unsrat.ac.id/v3/index.php/semnas-sinta/article/view/53999

Zulkifli, Dharmawan IB. Analisa Pengaruh Perlakuan Alkalisasi Dan Hydrogen Peroksida Terhadap Kekuatan Mekanik Komposit Serat Sabut Kelapa Bermatriks Epoxy. J Polimesin. 2019;(Vol 17, No 1 (2019): Polimesin):41–6. http://dx.doi.org/10.30811/jpl.v17i1.844.

Wardhana AS, Hidalgo AM, Puspitasari D, Erlita I, Sitepu A. Compressive Strength of Ca(OH)2 Combined with Musa Acuminata as a Pulp Capping Material. Dentino Jurnal Kedokteran Gigi. 2024; 9(1); 47-51. http://dx.doi.org/10.20527/dentino.v9i1.18861

Pangabdian, F., Hadinata, Y., Emilda, Y., Cevanti, T. A., Soesil, D., & Faradila, R. A. (2025). Mechanical strength comparison of natural resources composite resin with coconut coir (Cocos nucifera L.) particulate fiber 70% cellulose filler and RMGIC. IOP Conference Series: Earth and Environmental Science, 1473(1), 012051. https://doi.org/10.1088/1755-1315/1473/1/012051

Sun G, Margaretta DL. Pengaruh Obat Kumur Mengandung Alkohol 9% Dan Non-Alkohol Terhadap Kekuatan Tekan Resin Komposit Bulk-Fill (Penelitian). J Kedokt Gigi Terpadu. 2020;1(2):1–4.

Saeed G, Cement I, Mozartha M, Praziandithe M. Pengaruh Penambahan Hidroksiapatit dari Cangkang Telur Terhadap Kekuatan Tekan Glass Ionomer Cement. J B-Dent. 2015;2(1):75–81. https://doi.org/10.33854/JBDjbd.42

Karimzadeh A, R. Koloor SS, Ayatollahi MR, Bushroa AR, Yahya MY. Assessment of the Nano-Indentation Method in the Mechanical Characterization of Heterogeneous Nanocomposite Materials Using Experimental and Computational Approaches. Sci Rep [Internet]. 2019;9(1):1–14. Available from: http://dx.doi.org/10.1038/s41598-019-51904-4

Moheet IA, Luddin N, Rahman IA, Kannan TP, Nik Abd Ghani NR, Masudi SM. Modifications of Glass Ionomer Cement Powder by the Addition of Recently Fabricated Nano-Fillers and Their Effect on the Properties: A Review. Eur J Dent. 2019;13(3):470–7. DOI: 10.1055/s-0039-1693524

Güçlü ZA, Patat Ş, Coleman NJ. The Impact of Nano- and Micro-Silica on the Setting Time and Microhardness of Conventional Glass–Ionomer Cements. Dent J. 2024;12(3). https://doi.org/10.3390/dj12030054

Munasir, Sulton A, Triwikantoro, Zainuri M, Darminto. Synthesis of Silica Nanopowder Produced from Indonesian Natural Sand via the Alkalifusion Route. AIP Conf Proc. 2013;1555:28–31. https://doi.org/10.1063/1.4820986

Erawati Wulandari, Nadie Fatimatuzzahro, I Dewa Ayu Ratna Dewanti, Anita Faizah. Enhancement of Glass Ionomer Cement Hardness by Adding Gourami Scale Powder Nanoparticles. J Vocat Heal Stud. 2025;8(3):206–10. https://doi.org/10.20473/jvhs.V8.I3.2025.206-210

Hardyanti IS, Nurani I, Septyaningsih D, Hp H, Apriliani E, Prastyo EA, et al. Pemanfaatan Silika (SiO2) dan Bentonit sebagai Adsorben Logam Berat Fe pada Limbah Batik J Sains Terap. 2017;1(2):17–23.

AlTawaiha H, Alhomaidat F, Eljufout T. A Review of the Effect of Nano-Silica on the Mechanical and Durability Properties of Cementitious Composites. Infrastructures. 2023;8(9).

Rahman IAB, Masudi SM, Luddin N, Shiekh RA. One-pot Synthesis of Hydroxyapatite-Silica Nanopowder Composite for Hardness Enhancement of Glass-Ionomer- -Cement (GIC). Bulletin of Materials Science. 2014;37(2):213–9.

Utama MD, Ariani N, Machmud E, Mude AH, Dharma MAT, Taqwim A, et al. Synthesis and Application of Sol-Gel-Derived Nano-Silica in Glass Ionomer Cement for Dental Cementation. Biomimetics. 2025;10(4):1–12. https://doi.org/10.3390/biomimetics10040235

Murugan R, Yazid F, Nasruddin NS, Anuar NNM. Effects of Nanohydroxyapatite Incorporation into Glass Ionomer Cement (GIC). Minerals. 2022;12(1):1–10. https://doi.org/10.3390/min12010009

Elbatanony MM, El Shahawi AM. Evaluation of Some Mechanical and Optical Properties of Modified Glass Ionomer Cement with TiO2 and SiO2 Nanoparticles. Bull Natl Res Cent [Internet]. 2024;48(1). Available from: https://doi.org/10.1186/s42269-024-01263-6




DOI: http://dx.doi.org/10.20527/dentino.v11i2.26280

DOI (PDF): http://dx.doi.org/10.20527/dentino.v11i2.26280.g12537

Article Metrics

Abstract view : 32 times
PDF - 34 times

Refbacks



Creative Commons License
This work is licensed under a Creative Commons Attribution-ShareAlike 4.0 International License.

Contact Us:
Faculty of Dentistry
Lambung Mangkurat University
Jalan Veteran No. 128 B Banjarmasin, Indonesia

E-mail. [email protected]
Website. fkg.ulm.ac.id

 


Creative Commons License
This work is licensed under a Creative Commons Attribution 4.0 International License.